1. Importance of Food Safety With the escalation of environmental pollution, the problem of heavy metal and harmful element contamination in crops has become increasingly prominent. As a representative leafy vegetable crop, spinach is more prone to absorbing and enriching heavy metals from soil and the atmosphere through its roots and leaves due to its large leaf surface area and short growth cycle.
2. Health Risks Toxic elements such as lead (Pb), cadmium (Cd), arsenic (As), and thallium (Tl) can accumulate in the human body through the food chain, causing damage to multiple systems such as the nervous and renal systems. Standards such as the EU No 1881/2006 and China’s GB2762-2022 have set strict limits on elemental concentrations in vegetables.
3. Technical Needs Traditional atomic absorption spectrometry has issues such as low single-element detection efficiency and insufficient sensitivity. There is an urgent need to establish an efficient and accurate method for simultaneous multi-element detection.
Article Conclusion
1. In the analysis of spinach quality control sample GBW10015a, matrix effects were eliminated through internal standard and instrument parameter optimization. The excellent KED effect and application of electronic dilution ensured excellent trueness of impurity results for 19 elements, with 17 elements within the certified value range and the error of the other 2 elements within 10% of the median value.
2. This test demonstrates that the iQuad 2300 has strong matrix tolerance and quantification capabilities, enabling accurate and rapid quantification of elemental impurities and even major elements in green leafy vegetable samples.
Highlights of the Scheme
Nineteen elements were evaluated in this experiment. Seventeen elements fell within the certified value range, and the test results of the other two elements were within a 10% error range of the certified median values. Elements in trace to ultra-trace concentration ranges, and even the K element with percentage-level content, showed good trueness data. This fully meets the quality control requirements of food industry laboratories.
Building upon intelligent microwave digestion technology, the system integrates with an ICP-MS analytical platform to achieve complete end-to-end automation.
The fully automated process includes acid addition, sample loading, digestion, cooling, dilution, homogenization, sample solution transfer, and ICP-MS auto-triggered analysis, enabling high-throughput automated sample analysis.”
High analytical throughput
Fully automatic analysis of more than 200 samples per day
Three independent microwave oven cavities can run three different heating programs at the same time, which can increase the work efficiency by 10 times and greatly speed up the scientific research process.
Robust analytical performance
The microwave robot has 96 sample positions, and each digestion tank can withstand 45 Bar pressure and 240°C temperature, which truly realizes high-pressure and high-throughput microwave digestion and has strong sample processing capabilities.
The ICP-MS part is well-known in the industry for its “robust performance”. Its long-term stability and collision cell have strong performance in reducing interference, and its performance is impressive.
Remote monitoring, unattended operation
2300P has remote monitoring function. Users can monitor the instrument remotely through mobile phone APP to reduce manpower and realize unattended work.